BF9101 DFAA DATA Revised 9/8/92 From Calib 11/91 Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Average ß1 Actual n 12 15 12 15 15 15 12 12 12 13 13 12 11 9 Mean X 8.6143462 9.5250195 8.4195733 7.6196442 21.7327967 6.7667079 8.1703398 8.01386588 8.3330761 7.90386128 7.83370148 7.85603796 9.51769305 11.8548525 Sxx 490.86 648.324 490.86 648.324 5834.916 648.324 490.86 490.86 490.86 551.423077 551.423077 490.86 434.307273 283.5 ß1 756.819 777.951 762.351 620.878 523.09 745.03 847.415 675.226 846.496 947.006 741.491 1030.853 877.61 124.122 731.845154 t(.025,n-2) 2.228 2.16 2.228 2.16 2.16 2.16 2.228 2.228 2.228 2.201 2.201 2.228 2.262 2.365 Std. Error 168.753 193.963 281.411 288.606 275.278 1183.787 180.68 199.168 127.503 145.32 107.014 358.681 957.307 93.36 c^2 0.0005028 0.00044735 0.00137799 0.00155494 0.00022144 0.01816833 0.00045973 0.00087986 0.00022944 0.00020687 0.00018299 0.00122432 0.01401804 0.01116178 latitude: 31° 51.5'N Extra amines longitude: 80° 53.0'W Asp-Lys sample depth: 3 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 1MA 1422 2892 7921 2589 4755 2756 125 125 125 421 125 125 125 927 12222 1MB 1082 2973 6551 2687 4586 1898 125 125 125 685 125 125 125 819 10553 1MC 1264 3247 6169 1552 5980 2240 125 837 125 345 125 125 125 125 13404 Area Mean 1256 3037.33 6880.33 2276 5107 2298 125 362.33 125 483.67 125 125 125 623.67 12059.67 Area Std. Error 98.23 107.41 531.89 363.1 439.22 249.38 0 237.33 0 103.03 0 0 0 251.27 827.01 Predicted Conc.(nM) 1.66 3.9 9.03 3.67 9.76 3.08 0.15 0.54 0.15 0.51 0.17 0.12 0.14 5.02 28.88 16.48 45.36 63.67 Lower 95% 1.34 3.58 7.45 2.37 7.92 1.89 0.02 -0.27 0.06 0.26 0.09 -0.09 -0.64 0.1 Upper 95% 1.97 4.23 10.6 4.95 11.6 4.14 0.27 1.33 0.23 0.76 0.25 0.31 0.66 9.79 latitude: 31° 49.0'N Extra amines longitude: 80° 48.0'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 2MA 3155 2492 7179 12317 10981 4104 1060 125 125 1371 658 125 125 1326 9751 2MB 827 2190 6062 2300 4676 1463 125 125 125 809 125 125 125 924 10946 2MC 1463 2231 6111 3935 5847 2780 450 125 125 1163 296 125 125 125 9822 Area Mean 1815 2304.33 6450.67 6184 7168 2782.33 545 125 125 1114.33 359.67 125 125 791.67 10173 Area Std. Error 694.7 94.58 364.44 3102.61 1936.24 762.39 274.06 0 0 164.05 157.12 0 0 352.96 387.04 Predicted Conc. (nM) 2.4 2.96 8.46 9.96 13.7 3.73 0.64 0.19 0.15 1.18 0.49 0.12 0.14 6.38 42.04 13.9 55.94 75.15 Lower 95% 0.35 2.67 7.37 -0.84 5.7 1.29 -0.09 0.01 0.06 0.78 0.01 -0.09 -0.64 -0.47 Upper 95% 4.44 3.25 9.55 20.77 21.7 6.07 1.37 0.35 0.23 1.57 0.96 0.31 0.66 13.1 latitude: 31° 46.0'N Extra amines longitude: 80° 43.0'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 3MA 1831 2117 6150 7109 7594 2951 370 125 125 962 303 125 125 850 7948 3MB 620 1669 5532 1366 3126 1010 125 125 125 125 125 125 125 1408 5444 3MC 909 1762 5260 1772 4476 1580 125 125 125 469 125 125 125 1480 8111 Area Mean 1120 1849.33 5647.33 3415.67 5065.33 1847 206.67 125 125 518.67 184.33 125 125 1246 7167.67 Area Std. Error 365.16 136.5 263.31 1850.38 1323.03 576 81.67 0 0 242.89 59.33 0 0 199.09 863.12 Predicted Conc. (nM) 1.48 2.38 7.41 5.5 9.68 2.48 0.24 0.19 0.15 0.55 0.25 0.12 0.14 10.04 33.2 9.79 42.99 77.22 Lower 95% 0.39 1.97 6.6 -0.95 4.21 0.51 -0.01 0.01 0.06 -0.02 0.05 -0.09 -0.64 6.16 Upper 95% 2.56 2.77 8.21 11.95 15.15 4.29 0.49 0.35 0.23 1.12 0.44 0.31 0.66 13.88 latitude: 31° 40.0'N Extra amines longitude: 80° 33.0'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 4MA 2521 2420 7431 14741 15803 5984 973 884 125 2092 469 125 125 1073 11858 4MB 3012 2328 6229 14947 15515 6134 808 776 125 1691 484 125 125 125 12926 4MC 3070 2533 7975 15224 15499 6135 782 125 125 1719 416 125 125 980 13514 Area Mean 2867.67 2427 7211.67 14970.7 15605.67 6084.33 854.33 595 125 1834 456.33 125 125 726 12766 Area Std. Error 174.14 59.28 515.82 139.93 98.77 50.17 59.81 237.06 0 129.25 20.63 0 0 301.7 484.69 Predicted Conc. (nM) 3.79 3.12 9.46 24.11 29.83 8.17 1.01 0.88 0.15 1.94 0.62 0.12 0.14 5.85 79.72 17.44 97.17 82.05 Lower 95% 3.26 2.91 7.93 23.56 29.33 7.27 0.8 0.07 0.06 1.62 0.51 -0.09 -0.64 -0.02 Upper 95% 4.32 3.33 10.99 24.71 30.34 9.11 1.21 1.68 0.23 2.25 0.72 0.31 0.66 11.59 latitude: 31° 35.7'N Extra amines longitude: 80° 22.9'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 5MA 376 1613 6134 1201 2639 959 125 320 125 790 125 125 125 979 6600 5MB 455 1630 6072 1217 4564 2028 303 125 643 939 323 125 125 772 10678 5MC 629 1494 6342 1215 2063 767 125 125 125 125 125 125 125 1799 6893 Area Mean 486.67 1579 6182.67 1211 3088.67 1251.33 184.33 190 297.67 618 191 125 125 1183.33 8057 Area Std. Error 74.73 42.78 81.65 5.03 756.17 392.27 59.33 65 172.67 250.22 66 0 0 313.58 1313.23 Predicted Conc. (nM) 0.64 2.03 8.11 1.95 5.9 1.68 0.22 0.28 0.35 0.65 0.26 0.12 0.14 9.53 23.77 11.01 34.77 68.34 Lower 95% 0.38 1.85 7.77 1.7 2.77 0.16 0.02 0 -0.11 0.06 0.04 -0.09 -0.64 3.47 Upper 95% 0.89 2.2 8.45 2.18 9.04 3.01 0.41 0.55 0.81 1.24 0.47 0.31 0.66 15.54 5MAm 2992 2456 6193 11241 9077 2999 719 125 125 1308 649 125 125 508 6215 5MBm 1282 2140 5158 5407 6415 2327 602 125 125 1170 598 125 125 856 7328 5MCm 1260 1406 7095 6185 7218 2001 868 125 125 1094 380 125 125 285 7176 Area Mean 1844.67 2000.67 6148.67 7611 7570 2442.33 729.67 125 125 1190.67 542.33 125 125 549.67 6906.33 Area Std. Error 573.7 311.01 559.6 1828.84 788.35 293.81 76.97 0 0 62.63 82.49 0 0 166.14 348.44 Predicted Conc. (nM) 2.44 2.57 8.07 12.26 14.47 3.28 0.86 0.19 0.15 1.26 0.73 0.12 0.14 4.43 42.89 9.44 52.33 81.97 Lower 95% 0.74 1.7 6.41 5.89 11.2 2 0.62 0.01 0.06 1.09 0.47 -0.09 -0.64 1.12 Upper 95% 4.13 3.44 9.72 18.64 17.74 4.43 1.1 0.35 0.23 1.43 0.99 0.31 0.66 7.57 5MAn 773 1883 9137 2054 1844 681 125 125 125 125 125 125 125 125 4947 5MBn 670 1366 4732 1205 2016 554 518 125 125 364 125 125 125 125 4592 5MCn 979 125 8694 2036 2684 857 392 125 125 125 125 125 125 125 4771 Area Mean 807.33 1124.67 7521 1765 2181.33 697.33 345 125 125 204.67 125 125 125 125 4770 Area Std. Error 90.84 521.64 1400.35 280.05 256.19 87.85 115.86 0 0 79.67 0 0 0 0 102.48 Predicted Conc. (nM) 1.07 1.45 9.87 2.84 4.17 0.94 0.41 0.19 0.15 0.22 0.17 0.12 0.14 1.01 12.86 6.52 19.37 66.36 Lower 95% 0.77 -0.01 5.76 1.83 3.07 -0.04 0.07 0.01 0.06 0.01 0.09 -0.09 -0.64 0.4 Upper 95% 1.36 2.9 13.97 3.84 5.26 1.7 0.73 0.35 0.23 0.42 0.25 0.31 0.66 1.37 latitude: 31° 30.6'N Extra amines longitude: 80° 11.8'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 6SA --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 6SB 850 1511 7773 3462 4554 1758 125 125 125 1101 125 125 125 957 7668 6SC 558 1251 6049 1081 3637 965 125 125 125 494 125 125 125 909 7362 Area Mean 704 1381 6911 2271.5 4095.5 1361.5 125 125 125 797.5 125 125 125 933 7515 Area Std. Error 146 130 862 1190.5 458.5 396.5 0 0 0 303.5 0 0 0 24 153 Predicted Conc. (nM) 0.93 1.78 9.07 3.66 7.83 1.83 0.15 0.19 0.15 0.84 0.17 0.12 0.14 7.52 25.29 10.27 35.56 71.12 Lower 95% 0.48 1.39 6.53 -0.5 5.91 0.3 0.02 0.01 0.06 0.13 0.09 -0.09 -0.64 6.75 Upper 95% 1.38 2.15 11.6 7.8 9.74 3.17 0.27 0.35 0.23 1.55 0.25 0.31 0.66 8.19 latitude: 31° 30.6'N Extra amines longitude: 80° 11.8'W Asp-Lys sample depth: 25 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 6BA 506 1151 5652 1652 2722 659 125 125 125 125 125 125 125 1415 3714 6BB 873 909 7691 3260 2877 933 125 125 125 125 125 125 125 983 6003 6BC 437 833 5415 1593 1965 570 125 125 125 125 125 125 125 1842 5025 Area Mean 605.33 964.33 6252.67 2168.33 2521.33 720.67 125 125 125 125 125 125 125 1413.33 4914 Area Std. Error 135.31 95.88 722.41 546.1 281.74 109.23 0 0 0 0 0 0 0 247.97 663.1 Predicted Conc. (nM) 0.8 1.24 8.2 3.49 4.82 0.97 0.15 0.19 0.15 0.13 0.17 0.12 0.14 11.39 23.75 6.71 30.46 77.96 Lower 95% 0.38 0.94 6.08 1.57 3.62 -0.03 0.02 0.01 0.06 0.05 0.09 -0.09 -0.64 6.59 Upper 95% 1.21 1.53 10.33 5.4 6.01 1.75 0.27 0.35 0.23 0.22 0.25 0.31 0.66 16.17 latitude: 31° 37.8'N Extra amines longitude: 80° 01.6'W Asp-Lys sample depth: 4 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 7MA 135978 41394 9214 266942 340122 189416 64508 8248 19161 102872 44432 125 125 2377 228999 7MB 139008 21649 8777 272196 330563 194136 65295 9113 19304 100845 43917 125 125 2472 250086 7MC 138248 44289 8291 288670 365443 201418 67216 8011 17630 107348 44438 125 125 ?11960 229390 Area Mean 137745 35777.3 8760.67 275936 345376 194990 65673 8457.33 18698.3 103688 44262.3 125 125 2424.5 236158.33 Area Std. Error 910.17 7113.43 266.57 6545.16 10406.04 3490.89 804.26 334.9 535.76 1921.12 172.68 0 0 47.5 6964.75 Predicted Conc. (nM) 182 45.99 11.49 444.43 660.26 261.72 77.5 12.53 22.09 109.49 59.69 0.12 0.14 19.53 1895.5 322.69 2218.19 85.45 Lower 95% 179.39 26.25 10.68 422.3 617.43 255.95 75.4 11.41 20.68 105.04 59.17 -0.09 -0.64 18.49 Upper 95% 184.79 65.76 12.31 467.91 703.38 276.92 79.66 13.65 23.51 113.98 60.23 0.31 0.66 20.75 7MAm 24888 7492 6916 93655 82450 37077 12851 1448 3505 18324 8236 125 125 1617 43525 7MBm 25702 6679 9026 99809 88726 37687 13398 520 3952 19367 9019 125 125 1865 44354 7MCm 24729 6081 7187 94927 82948 36013 13005 1129 2869 16325 6038 125 125 1591 41988 Area Mean 25106.3 6750.67 7709.67 96130.3 84708 36925.7 13084.7 1032.33 3442 18005.3 7764.33 125 125 1691 43289 Area Std. Error 301.35 408.89 662.8 1875.63 2014.14 489.13 162.85 272.22 314.22 892.49 892.27 0 0 87.32 693.12 Predicted Conc. (nM) 33.17 8.68 10.11 154.83 161.94 49.56 15.44 1.53 4.07 19.01 10.47 0.12 0.14 13.62 472.59 59.15 531.74 88.88 Lower 95% 32.28 7.53 8.16 148.51 153.64 48.44 14.99 0.61 3.23 16.94 7.82 -0.09 -0.64 11.86 Upper 95% 34.09 9.82 12.07 161.61 170.29 52.27 15.9 2.44 4.9 21.09 13.12 0.31 0.66 15.43 7MAn 87032 27695 6307 229550 271748 138890 44800 4284 11500 65396 28359 125 125 7512 135780 7MBn 86676 18940 9776 228614 268910 139204 44920 4248 11551 65387 27911 125 125 7470 134893 7MCn --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 86854 23317.5 8041.5 229082 270329 139047 44860 4266 11525.5 65391.5 28135 125 125 7491 135336.5 Area Std. Error 178 4377.5 1734.5 468 1419 157 60 18 25.5 4.5 224 0 0 21 443.5 Predicted Conc. (nM) 114.76 29.97 10.55 368.96 516.79 186.63 52.94 6.32 13.62 69.05 37.94 0.12 0.14 60.35 1457.61 184.93 1642.53 88.74 Lower 95% 114.22 17.82 5.47 367.71 511.03 187.86 52.7 6.12 13.49 68.92 37.27 -0.09 -0.64 59.86 Upper 95% 115.41 42.14 15.63 371.34 522.78 192.06 53.21 6.51 13.74 69.21 38.62 0.31 0.66 61.93 latitude: 31° 34.9'N Extra amines longitude: 80° 56.2'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 8MA 2074 1819 6775 9628 8149 3240 610 125 125 1344 475 125 125 911 8807 8MB 825 1838 7127 1726 4167 1464 488 125 125 345 125 125 125 1197 9949 8MC 851 1883 8638 3047 4368 1387 336 125 125 493 125 125 125 125 17844 Area Mean 1250 1846.67 7513.33 4800.33 5561.33 2030.33 478 125 125 727.33 241.67 125 125 744.33 12200 Area Std. Error 412.07 18.98 571.44 2443.77 1295.13 605.24 79.25 0 0 311.28 116.67 0 0 320.48 2841.19 Predicted Conc. (nM) 1.65 2.37 9.86 7.73 10.63 2.73 0.56 0.19 0.15 0.77 0.33 0.12 0.14 6 33.37 16.67 50.04 66.68 Lower 95% 0.43 2.23 8.17 -0.78 5.27 0.69 0.32 0.01 0.06 0.04 -0.03 -0.09 -0.64 -0.23 Upper 95% 2.87 2.51 11.55 16.24 15.99 4.61 0.8 0.35 0.23 1.5 0.68 0.31 0.66 12.09 latitude: 31° 29.9'N Extra amines longitude: 80° 45.8'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 9MA 976 2193 7877 2399 2752 1103 125 125 125 402 125 125 125 1030 7293 9MB 923 1579 6781 1510 2394 1670 125 125 125 355 125 125 125 964 9669 9MC 1543 1795 6487 1943 2680 882 125 125 125 125 125 125 125 125 10874 Area Mean 1147.33 1855.67 7048.33 1950.67 2608.67 1218.33 125 125 125 294 125 125 125 706.33 9278.67 Area Std. Error 198.42 179.82 422.94 256.66 109.33 234.67 0 0 0 85.58 0 0 0 291.29 1052.01 Predicted Conc. (nM) 1.52 2.39 9.25 3.14 4.99 1.64 0.15 0.19 0.15 0.31 0.17 0.12 0.14 5.69 20.58 12.68 33.26 61.88 Lower 95% 0.91 1.87 7.99 2.21 4.45 0.46 0.02 0.01 0.06 0.09 0.09 -0.09 -0.64 0.01 Upper 95% 2.11 2.9 10.51 4.06 5.52 2.62 0.27 0.35 0.23 0.53 0.25 0.31 0.66 11.23 latitude: 31° 24.9'N Extra amines longitude: 80° 36.4'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 10MA 1534 1097 5482 3654 3027 1014 301 125 125 125 125 125 125 1704 5658 10MB 636 1863 8493 9941 6998 2092 402 125 125 1972 125 125 125 615 50619 10MC 684 1552 5489 2371 2851 1175 125 125 125 125 125 125 125 398 7215 Area Mean 951.33 1504 6488 5322 4292 1427 276 125 125 740.67 125 125 125 905.67 21164 Area Std. Error 291.66 222.42 1002.5 2339.01 1353.95 335.73 80.93 0 0 615.67 0 0 0 404.05 14734.36 Predicted Conc. (nM) 1.26 1.93 8.51 8.57 8.21 1.92 0.33 0.19 0.15 0.78 0.17 0.12 0.14 7.3 31.05 28.92 59.97 51.78 Lower 95% 0.38 1.3 5.57 0.43 2.6 0.53 0.08 0.01 0.06 -0.65 0.09 -0.09 -0.64 -0.52 Upper 95% 2.12 2.56 11.45 16.72 13.8 3.12 0.57 0.35 0.23 2.21 0.25 0.31 0.66 15.01 latitude: 31° 19.9'N Extra amines longitude: 80° 26.9'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 11MA 3182 1429 6416 12181 10586 4350 627 125 125 1483 475 125 125 1530 5696 11MB 1482 1525 7193 8189 9668 3931 503 125 125 1064 262 125 125 823 6838 11MC 1184 1420 5980 6942 8094 3322 430 125 125 868 125 125 125 588 8065 Area Mean 1949.33 1458 6529.67 9104 9449.33 3867.67 520 125 125 1138.33 287.33 125 125 980.33 6866.33 Area Std. Error 622.31 33.6 354.75 1580.05 727.64 298.44 57.5 0 0 181.38 101.83 0 0 283.08 684.02 Predicted Conc. (nM) 2.58 1.87 8.57 14.66 18.06 5.19 0.61 0.19 0.15 1.2 0.39 0.12 0.14 7.9 53.07 9.38 62.45 84.98 Lower 95% 0.74 1.71 7.5 9.17 15.04 3.92 0.41 0.01 0.06 0.77 0.07 -0.09 -0.64 2.4 Upper 95% 4.41 2.03 9.63 20.18 21.08 6.4 0.81 0.35 0.23 1.63 0.7 0.31 0.66 13.31 latitude: 31° 14.0'N Extra amines longitude: 80° 16.0'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 12SA 941 912 7603 2262 3222 1305 125 125 125 317 125 125 125 1215 8045 12SB 541 1098 11206 1518 4492 2106 125 540 125 125 125 125 125 125 6957 12SC 679 125 8082 888 2904 1030 125 125 125 125 125 125 125 600 7622 Area Mean 720.33 711.67 8963.67 1556 3539.33 1480.33 125 263.33 125 189 125 125 125 646.67 7541.33 Area Std. Error 117.3 298.21 1129.66 397.09 485.1 322.75 0 138.33 0 64 0 0 0 315.52 316.66 Predicted Conc. (nM) 0.95 0.91 11.76 2.51 6.77 1.99 0.15 0.39 0.15 0.2 0.17 0.12 0.14 5.21 19.65 10.3 29.96 65.6 Lower 95% 0.58 0.07 8.45 1.09 4.74 0.63 0.02 -0.1 0.06 0.03 0.09 -0.09 -0.64 -0.93 Upper 95% 1.32 1.75 15.08 3.9 8.79 3.16 0.27 0.87 0.23 0.37 0.25 0.31 0.66 11.2 latitude: 31° 14.0'N Extra amines longitude: 80° 16.0'W Asp-Lys sample depth: 30 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 12BA 438 1052 7109 1510 2500 650 125 125 125 125 125 125 125 1018 5207 12BB 471 1454 6808 1166 2454 892 125 125 125 386 125 125 125 829 5426 12BC 2462 2868 5288 7638 6270 2309 464 125 125 566 125 125 125 1093 6899 Area Mean 1123.67 1791.33 6401.67 3438 3741.33 1283.67 238 125 125 359 125 125 125 980 5844 Area Std. Error 669.23 550.7 563.57 2102.35 1264.4 517.4 113 0 0 128.02 0 0 0 78.54 531.27 Predicted Conc. (nM) 1.48 2.3 8.4 5.54 7.15 1.72 0.28 0.19 0.15 0.38 0.17 0.12 0.14 7.9 27.52 7.99 35.51 77.51 Lower 95% -0.49 0.76 6.73 -1.79 1.92 -0.1 -0.04 0.01 0.06 0.07 0.09 -0.09 -0.64 6.25 Upper 95% 3.46 3.83 10.06 12.86 12.38 3.36 0.6 0.35 0.23 0.69 0.25 0.31 0.66 9.46 latitude: 31° 08.8'N Extra amines longitude: 80° 06.2'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 13SA 710 1600 4552 1355 3131 960 125 125 125 374 125 125 125 2028 8000 13SB 957 1701 8634 2167 3674 1535 125 125 125 268 125 125 125 1372 6349 13SC 941 2762 5655 1552 2700 1002 125 125 125 125 125 125 125 723 7028 Area Mean 869.33 2021 6280.33 1691.33 3168.33 1165.67 125 125 125 255.67 125 125 125 1374.33 7125.67 Area Std. Error 79.8 371.65 1219.15 244.54 281.79 185.06 0 0 0 72.14 0 0 0 376.72 479.1 Predicted Conc. (nM) 1.15 2.6 8.24 2.72 6.06 1.56 0.15 0.19 0.15 0.27 0.17 0.12 0.14 11.07 26.35 9.74 36.08 73.02 Lower 95% 0.88 1.55 4.66 1.83 4.85 0.47 0.02 0.01 0.06 0.08 0.09 -0.09 -0.64 3.82 Upper 95% 1.41 3.63 11.81 3.6 7.25 2.47 0.27 0.35 0.23 0.46 0.25 0.31 0.66 18.31 latitude: 31° 08.8'N Extra amines longitude: 80° 06.2'W Asp-Lys sample depth: 30 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 13BA 931 1182 6812 1952 3898 926 125 125 125 125 125 125 125 1085 4480 13BB 986 796 8230 2321 3182 767 125 125 125 331 125 125 125 795 6332 13BC 125 2287 5146 1950 3170 1170 125 125 125 1030 125 125 125 571 10006 Area Mean 680.67 1421.67 6729.33 2074.33 3416.67 954.33 125 125 125 495.33 125 125 125 817 6939.33 Area Std. Error 278.29 446.78 891.23 123.33 240.69 117.2 0 0 0 273.87 0 0 0 148.79 1623.86 Predicted Conc. (nM) 0.9 1.83 8.83 3.34 6.53 1.28 0.15 0.19 0.15 0.52 0.17 0.12 0.14 6.58 21.9 9.48 31.38 69.78 Lower 95% 0.07 0.58 6.21 2.84 5.49 0.28 0.02 0.01 0.06 -0.12 0.09 -0.09 -0.64 3.62 Upper 95% 1.73 3.07 11.45 3.83 7.56 2.08 0.27 0.35 0.23 1.16 0.25 0.31 0.66 9.42 latitude: 31° 04.4'N Extra amines longitude: 79° 55.5'W Asp-Lys sample depth: 5 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 14SA 885 1073 6346 2802 2959 1066 125 125 125 403 125 125 125 1426 5702 14SB 897 842 5544 2145 3005 1049 125 125 125 125 125 125 125 1037 5115 14SC 578 1732 6118 1925 2463 684 125 125 125 125 125 125 125 801 4894 Area Mean 786.67 1215.67 6002.67 2290.67 2809 933 125 125 125 217.67 125 125 125 1088 5237 Area Std. Error 104.39 266.64 238.59 263.44 173.51 124.6 0 0 0 92.67 0 0 0 182.22 241.09 Predicted Conc. (nM) 1.04 1.56 7.87 3.69 5.37 1.25 0.15 0.19 0.15 0.23 0.17 0.12 0.14 8.77 22.82 7.16 29.98 76.13 Lower 95% 0.7 0.81 7.14 2.73 4.59 0.24 0.02 0.01 0.06 0 0.09 -0.09 -0.64 5.19 Upper 95% 1.37 2.31 8.61 4.63 6.14 2.06 0.27 0.35 0.23 0.46 0.25 0.31 0.66 12.27 14SAm 7289 2520 7279 47148 41349 20110 4732 691 1088 6618 1712 125 125 1053 18969 14SBm 5612 1663 8431 54295 45862 20964 5028 125 1050 7045 2148 3061 125 541 15238 14SCm 7767 2487 8321 48646 43226 20643 4258 668 1018 6436 1522 125 125 409 17652 Area Mean 6889.33 2223.33 8010.33 50029.7 43479 20572.3 4672.67 494.67 1052 6699.67 1794 1103.67 125 667.67 17286.33 Area Std. Error 653.4 280.33 367.04 2176.07 1308.92 249.05 224.25 184.95 20.23 180.48 185.3 978.67 0 196.4 1092.46 Predicted Conc. (nM) 9.1 2.86 10.51 80.58 83.12 27.61 5.51 0.73 1.24 7.07 2.42 1.07 0.14 5.38 226.85 23.62 250.47 90.57 Lower 95% 7.17 2.07 9.41 73.1 77.72 26.69 4.91 0.09 1.14 6.64 1.86 -1.06 -0.64 1.51 Upper 95% 11.03 3.64 11.61 88.28 88.55 29.31 6.12 1.36 1.34 7.5 2.97 3.19 0.66 9.11 14SAn 524 125 8343 2437 2389 694 445 125 125 125 125 125 125 125 5680 14SBn 481 125 6606 2028 2341 825 125 125 125 125 125 125 125 125 4225 14SCn 620 125 5941 3081 2467 1008 125 125 125 125 125 125 125 125 4534 Area Mean 541.67 125 6963.33 2515.33 2399 842.33 231.67 125 125 125 125 125 125 125 4813 Area Std. Error 41.09 0 716.05 306.49 36.72 91.06 106.67 0 0 0 0 0 0 0 442.58 Predicted Conc. (nM) 0.72 0.16 9.13 4.05 4.59 1.13 0.27 0.19 0.15 0.13 0.17 0.12 0.14 1.01 12.82 6.58 19.4 66.1 Lower 95% 0.53 0.03 7.03 2.95 4.26 0.15 -0.04 0.01 0.06 0.05 0.09 -0.09 -0.64 0.4 Upper 95% 0.89 0.28 11.24 5.14 4.91 1.9 0.58 0.35 0.23 0.22 0.25 0.31 0.66 1.37 latitude: 31° 04.4'N Extra amines longitude: 79° 55.5'W Asp-Lys sample depth: 40 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 14BA 1312 1023 5284 3546 2989 1063 390 125 125 125 125 125 125 1002 5225 14BB 785 125 8596 1114 2865 606 125 125 125 294 125 125 125 125 4175 14BC 1081 1389 5873 4260 3101 1012 125 125 125 479 125 125 125 1147 4891 Area Mean 1059.33 845.67 6584.33 2973.33 2985 893.67 213.33 125 125 299.33 125 125 125 758 4763.67 Area Std. Error 152.52 375.5 1020.1 952.24 68.16 144.58 88.33 0 0 102.23 0 0 0 319.26 309.72 Predicted Conc. (nM) 1.4 1.09 8.64 4.79 5.71 1.2 0.25 0.19 0.15 0.32 0.17 0.12 0.14 6.11 21.62 6.51 28.13 76.86 Lower 95% 0.93 0.03 5.64 1.46 5.3 0.16 -0.01 0.01 0.06 0.06 0.09 -0.09 -0.64 -0.1 Upper 95% 1.86 2.13 11.63 8.11 6.11 2.03 0.51 0.35 0.23 0.57 0.25 0.31 0.66 12.18