BF9109 DFAA DATA Revised 9/8/92 From Revised Calib 11/91 Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Average ß1 Actual n 12 15 12 15 15 15 12 12 12 13 13 12 11 9 Corrected Mean X 8.6143462 9.5250195 8.4195733 7.6196442 21.7327967 6.7667079 8.1703398 8.01386588 8.3330761 7.90386128 7.83370148 7.85603796 9.51769305 11.8548525 Sxx 490.86 648.324 490.86 648.324 5834.916 648.324 490.86 490.86 490.86 551.423077 551.423077 490.86 434.307273 283.5 ß1 756.819 777.951 762.351 620.878 523.09 745.03 847.415 675.226 846.496 947.006 741.491 1030.853 877.61 124.122 731.8451539 t(.025,n-2) 2.228 2.16 2.228 2.16 2.16 2.16 2.228 2.228 2.228 2.201 2.201 2.228 2.262 2.365 Std. Error 168.753 193.963 281.411 288.606 275.278 1183.787 180.68 199.168 127.503 145.32 107.014 358.681 957.307 93.36 c^2 0.0005028 0.00044735 0.00137799 0.00155494 0.00022144 0.01816833 0.00045973 0.00087986 0.00022944 0.00020687 0.00018299 0.00122432 0.01401804 0.01116178 latitude: 31° 51.4'N longitude: 80° 52.8'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 1MC 2455 4269 8808 2347 5004 2055 914 524 ?303 ?303 125 125 125 1080 21131 Area Mean 2455 4269 8808 2347 5004 2055 914 524 #DIV/0! #DIV/0! 125 125 125 1080 21131 Predicted Conc. (nM) 3.24 5.49 11.55 3.78 9.57 2.76 1.08 0.78 #DIV/0! #DIV/0! 0.17 0.12 0.14 8.7 35.82 28.87 64.7 55.37 latitude: 32° 09.3'N longitude: 80° 30.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 2MB 1344 5192 11200 1128 7394 1782 1049 644 418 290 310 125 125 1084 18996 Area Mean 1344 5192 11200 1128 7394 1782 1049 644 418 290 310 125 125 1084 18996 Predicted Conc. (nM) 1.78 6.67 14.69 1.82 14.14 2.39 1.24 0.95 0.49 0.31 0.42 0.12 0.14 8.73 39.2 25.96 65.16 60.16 latitude: 32° 28.3'N longitude: 80° 07.2'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 3MA' 2433 8998 10898 1641 7677 2778 686 905 636 545 125 257 3569 125 15082 3MA" 3558 10764 9947 4817 15516 5168 1304 944 609 720 463 125 125 569 24993 Area Mean 2995.5 9881 10422.5 3229 11596.5 3973 995 924.5 622.5 632.5 294 191 1847 347 20037.5 Area Std. Error 562.5 883 475.5 1588 3919.5 1195 309 19.5 13.5 87.5 169 66 1722 222 4955.5 Predicted Conc. (nM) 3.96 12.7 13.67 5.2 22.17 5.33 1.17 1.37 0.74 0.67 0.4 0.19 2.1 2.8 58.79 27.38 86.17 68.23 Lower 95% 2.29 10.25 12.27 -0.34 5.98 1.7 0.35 1.18 0.64 0.45 -0.11 -0.07 -2.52 -1.59 Upper 95% 5.62 15.16 15.09 10.73 38.36 8.91 1.99 1.55 0.83 0.89 0.9 0.42 6.52 6.98 latitude: 32° 45.9'N longitude: 80° 35.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 4MB 1694 5217 10982 1213 5954 2403 1600 787 344 316 274 125 125 606 17919 4MC 2172 5075 9056 2074 9084 3500 930 849 125 563 125 125 125 629 17715 Area Mean 1933 5146 10019 1643.5 7519 2951.5 1265 818 234.5 439.5 199.5 125 125 617.5 17817 Area Std. Error 239 71 963 430.5 1565 548.5 335 31 109.5 123.5 74.5 0 0 11.5 102 Predicted Conc. (nM) 2.55 6.61 13.14 2.65 14.37 3.96 1.49 1.21 0.28 0.46 0.27 0.12 0.14 4.97 39.1 24.35 63.45 61.63 Lower 95% 1.83 6.37 10.32 1.12 7.9 2.09 0.6 1 -0.03 0.16 0.03 -0.09 -0.64 4.33 Upper 95% 3.27 6.85 15.98 4.16 20.84 5.73 2.38 1.41 0.58 0.76 0.5 0.31 0.66 5.47 latitude: 32° 41.4'N longitude: 79° 29.9'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 5MB 1843 3809 11250 3223 4976 2075 958 597 407 1257 431 125 125 661 75751 5MC 2115 3317 8230 1952 4070 1577 646 457 380 598 125 125 125 1154 19255 Area Mean 1979 3563 9740 2587.5 4523 1826 802 527 393.5 927.5 278 125 125 907.5 47503 Area Std. Error 136 246 1510 635.5 453 249 156 70 13.5 329.5 153 0 0 246.5 28248 Predicted Conc. (nM) 2.61 4.58 12.78 4.17 8.65 2.45 0.95 0.78 0.46 0.98 0.37 0.12 0.14 7.31 33.58 64.91 98.49 34.1 Lower 95% 2.19 3.88 8.36 1.94 6.75 1.25 0.51 0.49 0.37 0.21 -0.09 -0.09 -0.64 2.5 Upper 95% 3.03 5.27 17.21 6.39 10.54 3.49 1.37 1.06 0.56 1.75 0.83 0.31 0.66 12.02 latitude: 32° 35.0'N longitude: 79° 22.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 6MB 875 2320 8969 646 2796 997 125 435 125 125 125 125 125 1213 9498 6MC 1664 3229 9117 2399 4336 1636 125 579 125 125 125 125 125 125 11493 Area Mean 1269.5 2774.5 9043 1522.5 3566 1316.5 125 507 125 125 125 125 125 669 10495.5 Area Std. Error 394.5 454.5 74 876.5 770 319.5 0 72 0 0 0 0 0 544 997.5 Predicted Conc. (nM) 1.68 3.57 11.86 2.45 6.82 1.77 0.15 0.75 0.15 0.13 0.17 0.12 0.14 5.39 23.28 14.34 37.62 61.88 Lower 95% 0.5 2.29 11.54 -0.62 3.62 0.42 0.02 0.45 0.06 0.05 0.09 -0.09 -0.64 -5.12 Upper 95% 2.84 4.83 12.2 5.51 10.01 2.93 0.27 1.04 0.23 0.22 0.25 0.31 0.66 15.75 latitude: 32° 24.1'N longitude: 79° 09.7'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 7SB 710 1016 9255 1485 2453 948 125 125 276 256 125 125 125 758 8936 Area Mean 710 1016 9255 1485 2453 948 125 125 276 256 125 125 125 758 8936 Predicted Conc. (nM) 0.94 1.31 12.14 2.39 4.69 1.27 0.15 0.19 0.33 0.27 0.17 0.12 0.14 6.11 18.07 12.21 30.28 59.67 latitude: ? longitude: ? Extra amines sample depth: ? Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 7BB 1049 1742 9079 1523 3655 1366 557 125 125 125 125 125 125 462 17132 Area Mean 1049 1742 9079 1523 3655 1366 557 125 125 125 125 125 125 462 17132 Predicted Conc. (nM) 1.39 2.24 11.91 2.45 6.99 1.83 0.66 0.19 0.15 0.13 0.17 0.12 0.14 3.72 20.18 23.41 43.58 46.29 latitude: 32° 24.1'N longitude: 79° 09.7'W Extra amines sample depth: 30 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 8SB 836 1532 9925 855 2683 845 125 125 125 125 125 125 125 843 8979 8SC 1796 1087 9065 3433 3194 1760 564 749 292 572 125 125 125 790 7911 Area Mean 1316 1309.5 9495 2144 2938.5 1302.5 344.5 437 208.5 348.5 125 125 125 816.5 8445 Area Std. Error 480 222.5 430 1289 255.5 457.5 219.5 312 83.5 223.5 0 0 0 26.5 534 Predicted Conc. (nM) 1.74 1.68 12.45 3.45 5.62 1.75 0.41 0.65 0.25 0.37 0.17 0.12 0.14 6.58 22.92 11.54 34.46 66.51 Lower 95% 0.32 1.05 11.18 -1.05 4.52 0.08 -0.19 -0.4 0.01 -0.16 0.09 -0.09 -0.64 5.77 Upper 95% 3.15 2.31 13.74 7.94 6.71 3.24 0.99 1.68 0.48 0.89 0.25 0.31 0.66 7.26 latitude: 32° 13.7'N longitude: 78° 56.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 8BB 846 2060 9393 1078 3105 1051 486 359 125 267 125 125 125 462 9217 Area Mean 846 2060 9393 1078 3105 1051 486 359 125 267 125 125 125 462 9217 Predicted Conc. (nM) 1.12 2.65 12.32 1.74 5.94 1.41 0.57 0.53 0.15 0.28 0.17 0.12 0.14 3.72 18.54 12.59 31.13 59.55 latitude: 31° 49.5'N longitude: 79° 15.9'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 9SA' 709 2249 9149 1159 2509 894 125 125 125 125 125 125 125 125 8739 9SA" 1126 2209 9297 1343 2207 745 125 125 125 125 125 125 125 125 8167 Area Mean 917.5 2229 9223 1251 2358 819.5 125 125 125 125 125 125 125 125 8453 Area Std. Error 208.5 20 74 92 151 74.5 0 0 0 0 0 0 0 0 286 Predicted Conc. (nM) 1.21 2.87 12.1 2.01 4.51 1.1 0.15 0.19 0.15 0.13 0.17 0.12 0.14 1.01 13.75 11.55 25.3 54.35 Lower 95% 0.58 2.72 11.77 1.6 3.82 0.13 0.02 0.01 0.06 0.05 0.09 -0.09 -0.64 0.4 Upper 95% 1.84 3 12.43 2.41 5.19 1.86 0.27 0.35 0.23 0.22 0.25 0.31 0.66 1.37 latitude: 31° 49.5'N longitude: 79° 15.9'W Extra amines sample depth: 50 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 9BA' 862 1845 9918 718 3542 502 125 125 125 125 125 125 125 1100 8320 9BA" 505 2076 7926 1103 2899 639 125 125 125 125 125 125 125 125 8411 Area Mean 683.5 1960.5 8922 910.5 3220.5 570.5 125 125 125 125 125 125 125 612.5 8365.5 Area Std. Error 178.5 115.5 996 192.5 321.5 68.5 0 0 0 0 0 0 0 487.5 45.5 Predicted Conc. (nM) 0.9 2.52 11.7 1.47 6.16 0.77 0.15 0.19 0.15 0.13 0.17 0.12 0.14 4.93 17.79 11.43 29.22 60.88 Lower 95% 0.36 2.17 8.78 0.74 4.79 -0.2 0.02 0.01 0.06 0.05 0.09 -0.09 -0.64 -4.5 Upper 95% 1.44 2.86 14.63 2.17 7.51 1.51 0.27 0.35 0.23 0.22 0.25 0.31 0.66 14.21 latitude: 32° 00.0'N longitude: 79° 28.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 10SA" 1143 3225 13308 792 2478 663 125 279 125 125 125 125 125 125 8612 Area Mean 1143 3225 13308 792 2478 663 125 279 125 125 125 125 125 125 8612 Predicted Conc. (nM) 1.51 4.15 17.46 1.28 4.74 0.89 0.15 0.41 0.15 0.13 0.17 0.12 0.14 1.01 14.84 11.77 26.61 55.77 latitude: 32° 00.0'N longitude: 79° 28.5'W Extra amines sample depth: 30 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 10BA' 1446 3229 8828 500 3030 686 125 515 125 125 125 125 125 125 8187 Area Mean 1446 3229 8828 500 3030 686 125 515 125 125 125 125 125 125 8187 Predicted Conc. (nM) 1.91 4.15 11.58 0.81 5.79 0.92 0.15 0.76 0.15 0.13 0.17 0.12 0.14 1.01 16.21 11.19 27.4 59.17 latitude: 32° 11.0'N longitude: 79° 42.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 11MA" 1252 5456 9514 1847 3947 1092 489 125 125 768 125 125 125 125 12078 Area Mean 1252 5456 9514 1847 3947 1092 489 125 125 768 125 125 125 125 12078 Predicted Conc. (nM) 1.65 7.01 12.48 2.97 7.55 1.47 0.58 0.19 0.15 0.81 0.17 0.12 0.14 1.01 23.81 16.5 40.32 59.07 latitude: 32° 21.5'N longitude: 79° 55.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 12MA' 891 5597 9222 1412 3560 1394 125 125 125 125 125 125 125 125 12750 12MA" 1249 5293 9364 1275 3336 1311 125 125 125 405 125 125 125 125 9659 Area Mean 1070 5445 9293 1343.5 3448 1352.5 125 125 125 265 125 125 125 125 11204.5 Area Std. Error 179 152 71 68.5 112 41.5 0 0 0 140 0 0 0 0 1545.5 Predicted Conc. (nM) 1.41 7 12.19 2.16 6.59 1.82 0.15 0.19 0.15 0.28 0.17 0.12 0.14 1.01 21.18 15.31 36.49 58.05 Lower 95% 0.87 6.55 11.87 1.82 6.04 0.87 0.02 0.01 0.06 -0.06 0.09 -0.09 -0.64 0.4 Upper 95% 1.95 7.44 12.52 2.5 7.13 2.57 0.27 0.35 0.23 0.61 0.25 0.31 0.66 1.37 latitude: 32° 04.0'N longitude: 80° 22.0'W Extra amines sample depth: 7 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 13MB 631 2738 9256 688 4120 1336 125 125 125 125 125 125 125 125 9426 13MC 1376 2226 8389 1371 4559 1822 125 125 125 125 125 125 125 125 8303 Area Mean 1003.5 2482 8822.5 1029.5 4339.5 1579 125 125 125 125 125 125 125 125 8864.5 Area Std. Error 372.5 256 433.5 341.5 219.5 243 0 0 0 0 0 0 0 0 561.5 Predicted Conc. (nM) 1.33 3.19 11.57 1.66 8.3 2.12 0.15 0.19 0.15 0.13 0.17 0.12 0.14 1.01 18.64 12.11 30.75 60.61 Lower 95% 0.22 2.47 10.29 0.44 7.34 0.93 0.02 0.01 0.06 0.05 0.09 -0.09 -0.64 0.4 Upper 95% 2.43 3.91 12.87 2.86 9.24 3.14 0.27 0.35 0.23 0.22 0.25 0.31 0.66 1.37 latitude: 31° 52.0'N longitude: 80° 10.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 14MC 1090 2067 8227 1205 3656 1562 366 125 262 125 125 125 125 632 11038 Area Mean 1090 2067 8227 1205 3656 1562 366 125 262 125 125 125 125 632 11038 Predicted Conc. (nM) 1.44 2.66 10.79 1.94 6.99 2.1 0.43 0.19 0.31 0.13 0.17 0.12 0.14 5.09 21.71 15.08 36.79 59 latitude: 31° 41.5'N longitude: 79° 56.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 15MB 706 2492 --- 1290 3137 1181 422 377 497 396 125 125 125 1365 10894 15MC 890 1964 9944 1793 3219 1104 125 125 125 125 313 125 125 125 8632 Area Mean 798 2228 9944 1541.5 3178 1142.5 273.5 251 311 260.5 219 125 125 745 9763 Area Std. Error 92 264 #DIV/0! 251.5 41 38.5 148.5 126 186 135.5 94 0 0 620 1131 Predicted Conc. (nM) 1.05 2.86 13.04 2.48 6.08 1.53 0.32 0.37 0.37 0.28 0.3 0.12 0.14 6 21.91 13.34 35.25 62.15 Lower 95% 0.75 2.12 #DIV/0! 1.57 5.74 0.59 -0.09 -0.08 -0.13 -0.05 0 -0.09 -0.64 -5.96 Upper 95% 1.35 3.61 #DIV/0! 3.38 6.41 2.28 0.73 0.81 0.86 0.6 0.58 0.31 0.66 17.83 latitude: 31° 30.5'N longitude: 79° 43.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 16SB 1000 1656 8613 1249 2580 896 125 125 125 305 125 125 125 125 7890 16SC 1498 1582 8298 3365 4317 1900 125 125 125 656 125 125 125 1045 7963 Area Mean 1249 1619 8455.5 2307 3448.5 1398 125 125 125 480.5 125 125 125 585 7926.5 Area Std. Error 249 37 157.5 1058 868.5 502 0 0 0 175.5 0 0 0 460 36.5 Predicted Conc. (nM) 1.65 2.08 11.09 3.72 6.59 1.88 0.15 0.19 0.15 0.51 0.17 0.12 0.14 4.71 22.05 10.83 32.88 67.06 Lower 95% 0.9 1.91 10.57 0.02 2.99 0.09 0.02 0.01 0.06 0.09 0.09 -0.09 -0.64 -4.2 Upper 95% 2.39 2.24 11.62 7.4 10.19 3.48 0.27 0.35 0.23 0.92 0.25 0.31 0.66 13.46 latitude: 31° 30.5'N longitude: 79° 43.5'W Extra amines sample depth: 35 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 16BB 835 1280 8354 805 2787 863 125 348 ?633 ?633 125 125 125 996 8193 Area Mean 835 1280 8354 805 2787 863 125 348 #DIV/0! #DIV/0! 125 125 125 996 8193 Predicted Conc. (nM) 1.1 1.65 10.96 1.3 5.33 1.16 0.15 0.52 #DIV/0! #DIV/0! 0.17 0.12 0.14 8.02 19.65 11.19 30.85 63.71 latitude: 31° 49.0'N longitude: 80° 57.0'W Extra amines sample depth: 3 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 17MA 2522 6674 9098 2090 7629 3389 1397 783 535 459 677 125 125 730 17338 17MA' 2127 8647 8067 1168 5162 2079 1203 650 ?361 ?361? 349 125 125 125 17636 17MA" 3416 13120 8845 1998 8809 3589 1410 1051 125 657 357 125 125 125 29473 Area Mean 2688.33 9480.33 8670 1752 7200 3019 1336.67 828 330 558 461 125 125 326.67 21482.33 Area Std. Error 381.28 1906.88 310.22 293.21 1074.43 473.53 66.94 117.93 205 99 108.02 0 0 201.67 3996.26 Predicted Conc. (nM) 3.55 12.19 11.37 2.82 13.76 4.05 1.58 1.23 0.39 0.59 0.62 0.12 0.14 2.63 43.68 29.35 73.03 59.81 Lower 95% 2.42 6.89 10.44 1.76 9.32 2.37 1.36 0.79 -0.16 0.34 0.29 -0.09 -0.64 -1.37 Upper 95% 4.68 17.49 12.32 3.86 18.21 5.64 1.79 1.65 0.93 0.83 0.95 0.31 0.66 6.42 latitude: 31° 46.5'N longitude: 80° 53.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 18MA 1750 5241 10047 1275 5050 2033 1030 563 450 330 125 125 125 125 14212 18MA' 1867 9548 8329 1047 5621 2657 1415 926 ?365 ?365 254 125 125 125 16381 18MA" 3042 12991 12125 2321 13462 2795 1495 1503 125 477 564 125 125 125 20522 Area Mean 2219.67 9260 10167 1547.67 8044.33 2495 1313.33 997.33 287.5 403.5 314.33 125 125 125 17038.33 Area Std. Error 412.55 2241.86 1097.45 392.23 2713.84 234.41 143.54 273.69 162.5 73.5 130.27 0 0 0 1850.95 Predicted Conc. (nM) 2.93 11.9 13.34 2.49 15.38 3.35 1.55 1.48 0.34 0.43 0.42 0.12 0.14 1.01 41.54 23.28 64.82 64.09 Lower 95% 1.71 5.68 10.12 1.1 4.17 2.19 1.15 0.55 -0.1 0.23 0.03 -0.09 -0.64 0.4 Upper 95% 4.15 18.13 16.56 3.87 26.59 4.38 1.94 2.39 0.77 0.62 0.82 0.31 0.66 1.37 latitude: 31° 39.5'N longitude: 80° 53.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 19MA 1046 3808 11784 782 3992 1292 125 461 454 125 125 125 125 749 11789 19MA' 2195 5156 9469 2302 4508 1374 708 487 125 257 261 125 125 125 9961 19MA" 937 5435 8871 1057 4172 1219 352 125 125 125 125 125 125 125 17337 Area Mean 1392.67 4799.67 10041.3 1380.33 4224 1295 395 357.67 234.67 169 170.33 125 125 333 13029 Area Std. Error 402.4 502.33 888.27 467.62 151.21 44.77 169.67 116.58 109.67 44 45.33 0 0 208 2217.7 Predicted Conc. (nM) 1.84 6.17 13.17 2.22 8.08 1.74 0.47 0.53 0.28 0.18 0.23 0.12 0.14 2.68 24.67 17.8 42.48 58.09 Lower 95% 0.64 4.77 10.57 0.57 7.38 0.8 0 0.1 -0.03 0.04 0.07 -0.09 -0.64 -1.44 Upper 95% 3.03 7.57 15.79 3.86 8.76 2.49 0.93 0.94 0.58 0.31 0.38 0.31 0.66 6.6 latitude: 31° 29.5'N longitude: 80° 34.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 20SA 855 2404 10357 950 2879 973 578 125 291 306 125 258 125 1366 11342 20SA' 1315 4364 6568 1773 3129 ?817 ?817 533 ?390 ?390 416 125 125 125 11501 20SA" 1970 4113 8409 4253 6968 2386 849 125 125 542 323 125 125 125 12879 Area Mean 1380 3627 8444.67 2325.33 4325.33 1679.5 713.5 261 208 424 288 169.33 125 538.67 11907.33 Area Std. Error 323.51 615.78 1093.94 992.68 1323.3 706.5 135.5 136 83 118 85.81 44.33 0 413.67 488 Predicted Conc. (nM) 1.82 4.66 11.08 3.75 8.27 2.25 0.84 0.39 0.25 0.45 0.39 0.16 0.14 4.34 27.71 16.27 43.98 63.01 Lower 95% 0.86 2.94 7.87 0.27 2.79 -0.06 0.46 -0.1 0.01 0.16 0.12 -0.07 -0.64 -3.69 Upper 95% 2.78 6.38 14.29 7.2 13.74 4.4 1.22 0.86 0.48 0.73 0.65 0.38 0.66 12.2 latitude: 31° 29.5'N longitude: 80° 34.0'W Extra amines sample depth: 15 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 20BA 1513 4109 9641 1099 3963 1306 615 542 301 125 125 125 125 1081 12460 20BA' 2000 4945 7400 2723 4567 ?743 ?743 356 ?409 ?409 125 125 125 125 12890 20BA" 1555 4786 8632 829 5246 1184 708 338 125 434 729 125 125 125 57309 Area Mean 1689.33 4613.33 8557.67 1550.33 4592 1245 661.5 412 213 279.5 326.33 125 125 443.67 27553 Area Std. Error 155.81 256.31 647.99 591.49 370.58 61 46.5 65.21 88 154.5 201.33 0 0 318.67 14878.52 Predicted Conc. (nM) 2.23 5.93 11.23 2.5 8.78 1.67 0.78 0.61 0.25 0.3 0.44 0.12 0.14 3.57 27.32 37.65 64.97 42.06 Lower 95% 1.75 5.2 9.32 0.42 7.22 0.72 0.6 0.33 0 -0.08 -0.16 -0.09 -0.64 -2.65 Upper 95% 2.71 6.65 13.14 4.56 10.33 2.43 0.95 0.88 0.5 0.66 1.04 0.31 0.66 9.61 latitude: 31° 18.5'N longitude: 80° 20.5'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 21SA" 1976 2415 9144 2817 4390 1535 477 523 125 371 125 125 125 125 8084 Area Mean 1976 2415 9144 2817 4390 1535 477 523 125 371 125 125 125 125 8084 Predicted Conc. (nM) 2.61 3.1 11.99 4.54 8.39 2.06 0.56 0.77 0.15 0.39 0.17 0.12 0.14 1.01 24.02 11.05 35.07 68.5 latitude: 31° 18.5'N longitude: 80° 20.5'W Extra amines sample depth: 25 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 21BA' 917 3361 8623 952 4624 1088 846 125 125 125 125 125 125 125 9928 21BA" 966 4041 8822 995 3889 1040 263 125 125 125 125 125 125 125 11572 Area Mean 941.5 3701 8722.5 973.5 4256.5 1064 554.5 125 125 125 125 125 125 125 10750 Area Std. Error 24.5 340 99.5 21.5 367.5 24 291.5 0 0 0 0 0 0 0 822 Predicted Conc. (nM) 1.24 4.76 11.44 1.57 8.14 1.43 0.65 0.19 0.15 0.13 0.17 0.12 0.14 1.01 19.69 14.69 34.38 57.28 Lower 95% 1.09 3.8 11.06 1.31 6.59 0.49 -0.13 0.01 0.06 0.05 0.09 -0.09 -0.64 0.4 Upper 95% 1.39 5.71 11.83 1.81 9.68 2.17 1.43 0.35 0.23 0.22 0.25 0.31 0.66 1.37 latitude: 31° 07.0'N longitude: 80° 07.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 22SA' 744 2659 9040 1050 3038 833 125 125 125 125 125 125 125 125 6125 22SA" 1405 2172 9215 1829 2627 925 125 125 125 125 125 125 125 125 9607 Area Mean 1074.5 2415.5 9127.5 1439.5 2832.5 879 125 125 125 125 125 125 125 125 7866 Area Std. Error 330.5 243.5 87.5 389.5 205.5 46 0 0 0 0 0 0 0 0 1741 Predicted Conc. (nM) 1.42 3.1 11.97 2.32 5.41 1.18 0.15 0.19 0.15 0.13 0.17 0.12 0.14 1.01 15.49 10.75 26.24 59.04 Lower 95% 0.43 2.41 11.62 0.93 4.52 0.23 0.02 0.01 0.06 0.05 0.09 -0.09 -0.64 0.4 Upper 95% 2.4 3.79 12.33 3.69 6.31 1.92 0.27 0.35 0.23 0.22 0.25 0.31 0.66 1.37 latitude: 30° 57.0'N longitude: 79° 53.5'W Extra amines sample depth: 10 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 23MA' 841 1258 10042 1085 40165 654 475 125 125 125 125 125 125 125 7857 23MA" 1124 1251 8621 1229 1443 481 125 125 125 125 125 125 125 125 6050 Area Mean 982.5 1254.5 9331.5 1157 20804 567.5 300 125 125 125 125 125 125 125 6953.5 Area Std. Error 141.5 3.5 710.5 72 19361 86.5 175 0 0 0 0 0 0 0 903.5 Predicted Conc. (nM) 1.3 1.61 12.24 1.86 39.77 0.76 0.35 0.19 0.15 0.13 0.17 0.12 0.14 1.01 47.57 9.5 57.07 83.35 Lower 95% 0.86 1.48 10.15 1.51 -40.18 -0.22 -0.13 0.01 0.06 0.05 0.09 -0.09 -0.64 0.4 Upper 95% 1.73 1.74 14.34 2.2 119.73 1.52 0.83 0.35 0.23 0.22 0.25 0.31 0.66 1.37 latitude: 31° 20.0'N longitude: 80° 55.0'W Extra amines sample depth: 5 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 24MA 1124 2768 10297 907 3135 994 125 394 449 125 125 125 125 1156 9114 24MA' 2883 4172 9184 4644 5406 2568 695 594 125 355 296 125 125 125 10477 24MB 1886 2451 8951 2043 3857 988 480 125 125 125 125 125 125 923 9707 Area Mean 1964.33 3130.33 9477.33 2531.33 4132.67 1516.67 433.33 371 233 201.67 182 125 125 734.67 9766 Area Std. Error 509.29 528.81 415.32 1106.07 669.91 525.67 166.19 135.88 108 76.67 57 0 0 312.17 394.57 Predicted Conc. (nM) 2.6 4.02 12.43 4.08 7.9 2.04 0.51 0.55 0.28 0.21 0.25 0.12 0.14 5.92 28.61 13.34 41.95 68.19 Lower 95% 1.09 2.55 11.2 0.21 5.12 0.19 0.05 0.06 -0.02 0.01 0.06 -0.09 -0.64 -0.15 Upper 95% 4.1 5.5 13.68 7.93 10.68 3.7 0.96 1.02 0.57 0.41 0.43 0.31 0.66 11.86 latitude: 31° 26.0'N longitude: 81° 01.5'W Extra amines sample depth: 7 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 25MA 875 4188 6079 1731 3941 1138 125 125 125 383 125 125 125 125 5461 25MB 1951 4862 8298 1462 4161 1695 125 663 ?592 ?592 125 125 125 125 14749 25MC 1962 3512 10326 1576 5414 1831 870 874 364 407 125 125 125 764 17547 Area Mean 1596 4187.33 8234.33 1589.67 4505.33 1554.67 373.33 554 244.5 395 125 125 125 338 12585.67 Area Std. Error 360.51 389.71 1226.42 77.95 458.75 212 248.33 222.98 119.5 12 0 0 0 213 3652.76 Predicted Conc. (nM) 2.11 5.38 10.8 2.56 8.61 2.09 0.44 0.82 0.29 0.42 0.17 0.12 0.14 2.72 25.87 17.2 43.07 60.07 Lower 95% 1.04 4.29 7.21 2.19 6.69 0.95 -0.23 0.06 -0.04 0.33 0.09 -0.09 -0.64 -1.49 Upper 95% 3.18 6.47 14.4 2.92 10.53 3.05 1.1 1.57 0.61 0.51 0.25 0.31 0.66 6.73 latitude: 31° 30.0'N longitude: 81° 05.5'W Extra amines sample depth: 2 m Asp-Lys Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nm) except 8AAA Total amines(nm) %known 26MA 2443 6535 12159 1309 6680 2471 1308 677 125 125 125 125 125 1392 27030 26MB 2471 5435 10271 1924 13473 2994 1549 596 677 527 125 125 125 1722 17272 26MC 2576 5710 8861 1833 8424 2266 1280 704 280 372 125 125 125 898 21521 Area Mean 2496.67 5893.33 10430.3 1688.67 9525.67 2577 1379 659 360.67 341.33 125 125 125 1337.33 21941 Area Std. Error 40.48 330.51 955.38 191.64 2036.87 216.74 85.38 32.45 164.37 117.06 0 0 0 239.43 2824.71 Predicted Conc. (nM) 3.3 7.58 13.68 2.72 18.21 3.46 1.63 0.98 0.43 0.36 0.17 0.12 0.14 10.77 49.86 29.98 79.84 62.45 Lower 95% 3.12 6.65 10.88 2 9.79 2.33 1.37 0.77 -0.02 0.07 0.09 -0.09 -0.64 6.14 Upper 95% 3.48 8.5 16.49 3.42 26.63 4.47 1.88 1.17 0.87 0.64 0.25 0.31 0.66 15.39