BF9203 DFAA DATA Revised 8/21/92 From Calib 3/92 Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Average ß1 Actual n 13 14 9 15 15 13 13 12 12 12 12 13 13 7 Corrected Mean X 9.525638335 10.20086894 10.73603293 11.18343035 25.07058018 8.980243525 8.828065412 9.713350937 9.06844642 9.504553971 9.360590794 10.7350849 12.34729046 12.20763176 Sxx 680.769231 744.857143 350 800.4 7203.6 680.769231 680.769231 606 606 606 606 787.692308 787.692308 369.428571 ß1 610.659661 647.136747 367.133333 470.565217 447.047226 929.690395 667.530169 581.793729 626.191419 833.240924 586.278878 692.975781 502.190527 107.110982 592.4932042 t(.025,n-2) 2.201 2.179 2.365 2.16 2.16 2.201 2.201 2.228 2.228 2.228 2.228 2.201 2.201 2.571 Std. Error 534.090397 572.727424 391.890048 1173.796799 1657.441626 967.792874 230.337886 471.016335 417.288714 642.906661 323.3255 488.535359 1353.923814 287.891455 c^2 0.005443412 0.004992813 0.018208538 0.036269922 0.00890282 0.007711313 0.000847284 0.005368978 0.003637616 0.004876547 0.002491318 0.003056605 0.044702818 0.129259723 latitude: 31° 51.0'N Extra amines longitude: 80° 48.0'W Asp-Lys sample depth: 3 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 1SA 2327 5512 3612 6129 6943 4298 955 1069 125 1012 125 2302 2039 125 6155 1SB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 1SC 1142 4691 3518 2516 4865 2803 668 125 125 664 125 2148 1820 125 6107 Area Mean 1734.50 5101.50 3565.00 4322.50 5904.00 3550.50 811.50 597.00 125.00 838.00 125.00 2225.00 1929.50 125.00 6131.00 Area Std. Error 592.50 410.50 47.00 1806.50 1039.00 747.50 143.50 472.00 0.00 174.00 0.00 77.00 109.50 0.00 24.00 Predicted Conc. (nM) 2.84 7.88 9.71 9.19 13.21 3.82 1.22 1.03 0.20 1.01 0.21 3.21 3.84 1.17 48.82 10.35 59.16 82.51 Lower 95% 0.60 6.40 8.80 0.55 7.66 1.90 0.70 -0.89 -0.22 0.31 -0.13 2.72 1.81 -2.91 Upper 95% 5.00 9.35 10.58 17.67 18.54 5.66 1.72 2.85 0.56 1.61 0.51 3.66 5.08 1.97 Mol % 5.82 16.15 19.89 18.82 27.05 7.82 2.49 2.10 0.41 2.06 0.44 6.58 7.87 36.87 latitude: 31° 46.0'N Extra amines longitude: 80° 43.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 2SA 1765 9830 2629 3392 5683 2389 637 125 125 655 125 2145 2302 125 7797 2SB 984 3731 3603 2407 5354 2368 125 125 125 697 125 2330 1784 125 7448 2SC 2252 4798 3339 7554 7510 3775 1066 1369 125 1203 125 3329 3187 125 6637 Area Mean 1667.00 6119.67 3190.33 4451.00 6182.33 2844.00 609.33 539.67 125.00 851.67 125.00 2601.33 2424.33 125.00 7294.00 Area Std. Error 369.31 1880.56 290.83 1577.34 670.59 465.54 272.00 414.67 0.00 176.08 0.00 367.73 409.60 0.00 343.60 Predicted Conc. (nM) 2.73 9.46 8.69 9.46 13.83 3.06 0.91 0.93 0.20 1.02 0.21 3.75 4.83 1.17 51.56 12.31 63.87 80.72 Lower 95% 1.27 3.08 6.59 1.89 9.88 1.75 -0.01 -0.78 -0.22 0.33 -0.13 2.49 2.06 -2.91 Upper 95% 4.12 15.82 10.72 16.90 17.58 4.27 1.82 2.54 0.56 1.64 0.51 4.97 6.89 1.97 Mol % 5.29 18.34 16.85 18.35 26.82 5.93 1.77 1.80 0.39 1.98 0.41 7.28 9.36 34.91 latitude: 31° 46.0'N Extra amines longitude: 80° 43.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 3SA 572 4757 4056 1233 3876 1351 426 125 125 125 125 2397 1734 125 6799 3SB 3380 5422 3717 10824 8815 6461 1542 2697 125 1257 478 2478 2021 125 9124 3SC --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 1976.00 5089.50 3886.50 6028.50 6345.50 3906.00 984.00 1411.00 125.00 691.00 301.50 2437.50 1877.50 125.00 7961.50 Area Std. Error 1404.00 332.50 169.50 4795.50 2469.50 2555.00 558.00 1286.00 0.00 566.00 176.50 40.50 143.50 0.00 1162.50 Predicted Conc. (nM) 3.24 7.86 10.59 12.81 14.19 4.20 1.47 2.43 0.20 0.83 0.51 3.52 3.74 1.17 56.17 13.44 69.61 80.70 Lower 95% -1.90 6.62 9.19 -9.60 1.94 -1.94 -0.38 -2.58 -0.22 -0.80 -0.25 3.07 1.65 -2.91 Upper 95% 8.30 9.08 11.97 35.34 26.26 10.27 3.32 7.35 0.56 2.37 1.24 3.92 5.02 1.97 Mol % 5.76 14.00 18.85 22.81 25.27 7.48 2.62 4.32 0.36 1.48 0.92 6.26 6.66 32.04 latitude: 31° 41.0'N Extra amines longitude: 80° 33.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 4SA 3223 5010 3528 10705 10787 6211 1653 1011 125 1555 423 2892 2575 125 7245 4SB 1237 2601 3604 2460 4765 1753 125 125 125 409 125 2186 1620 125 5521 4SC 2905 7885 3527 9099 8944 4435 1284 1877 125 1116 573 1820 1866 125 11880 Area Mean 2455.00 5165.33 3553.00 7421.33 8165.33 4133.00 1020.67 1004.33 125.00 1026.67 373.67 2299.33 2020.33 125.00 8215.33 Area Std. Error 615.88 1527.34 25.50 2523.62 1781.47 1295.74 460.33 505.77 0.00 333.82 131.66 314.61 286.28 0.00 1898.72 Predicted Conc. (nM) 4.02 7.98 9.68 15.77 18.27 4.45 1.53 1.73 0.20 1.23 0.64 3.32 4.02 1.17 64.32 13.87 78.18 82.26 Lower 95% 1.71 2.79 8.80 4.05 9.32 1.27 -0.01 -0.32 -0.22 0.19 0.02 2.22 1.61 -2.91 Upper 95% 6.27 13.15 10.51 27.84 27.09 7.55 3.05 3.68 0.56 2.20 1.21 4.37 5.65 1.97 Mol % 6.25 12.41 15.05 24.52 28.40 6.91 2.38 2.68 0.31 1.92 0.99 5.16 6.26 27.99 latitude: 31° 38.0'N Extra amines longitude: 80° 23.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 5SA 2644 11267 5045 5602 7032 3931 1526 1546 125 788 125 3248 5147 125 11702 5SB 621 3237 5214 2712 5577 1816 369 125 125 407 125 3298 5034 1307 10288 5SC 1522 15337 3930 3251 4857 1641 726 1467 298 626 125 1924 2152 125 19935 Area Mean 1595.67 9947.00 4729.67 3855.00 5822.00 2462.67 873.67 1046.00 182.67 607.00 125.00 2823.33 4111.00 519.00 13975.00 Area Std. Error 585.15 3554.78 402.80 887.25 639.71 735.90 342.06 461.06 57.67 110.39 0.00 449.90 980.04 394.00 3007.83 Predicted Conc. (nM) 2.61 15.37 12.88 8.19 13.02 2.65 1.31 1.80 0.29 0.73 0.21 4.07 8.19 4.85 63.29 23.59 86.88 72.85 Lower 95% 0.40 3.39 10.16 3.71 9.19 0.75 0.16 -0.08 -0.18 0.15 -0.13 2.57 3.31 -6.70 Upper 95% 4.75 27.41 15.68 12.45 16.64 4.45 2.45 3.59 0.70 1.23 0.51 5.54 12.68 14.21 Mol % 4.13 24.28 20.35 12.94 20.58 4.19 2.07 2.84 0.46 1.15 0.34 6.44 12.93 28.44 latitude: 31° 30.0'N Extra amines longitude: 80° 13.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 6SA --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 6SB 1690 4432 4032 5573 5097 2846 783 680 252 969 125 1944 1819 125 9410 6SC 1345 3560 3421 3345 3214 1482 704 918 125 706 423 2342 2031 125 5659 Area Mean 1517.50 3996.00 3726.50 4459.00 4155.50 2164.00 743.50 799.00 188.50 837.50 274.00 2143.00 1925.00 125.00 7534.50 Area Std. Error 172.50 436.00 305.50 1114.00 941.50 682.00 39.50 119.00 63.50 131.50 149.00 199.00 106.00 0.00 1875.50 Predicted Conc. (nM) 2.49 6.17 10.15 9.48 9.30 2.33 1.11 1.37 0.30 1.01 0.47 3.09 3.83 1.17 42.11 12.72 54.83 76.81 Lower 95% 1.65 4.60 7.98 4.02 4.15 0.55 0.87 0.67 -0.18 0.39 -0.21 2.32 1.81 -2.91 Upper 95% 3.24 7.71 12.30 14.80 14.16 4.00 1.34 1.99 0.72 1.54 1.10 3.82 5.06 1.97 Mol % 5.90 14.66 24.10 22.50 22.07 5.53 2.64 3.26 0.71 2.39 1.11 7.34 9.10 42.74 latitude: 31° 24.0'N Extra amines longitude: 80° 02.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 7SA 2664 4680 3847 7530 6284 3371 1415 125 125 667 125 1967 2117 125 2943 7SB 425 826 2286 1008 3144 845 125 125 125 125 125 1066 902 125 3839 7SC --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 1544.50 2753.00 3066.50 4269.00 4714.00 2108.00 770.00 125.00 125.00 396.00 125.00 1516.50 1509.50 125.00 3391.00 Area Std. Error 1119.50 1927.00 780.50 3261.00 1570.00 1263.00 645.00 0.00 0.00 271.00 0.00 450.50 607.50 0.00 448.00 Predicted Conc. (nM) 2.53 4.25 8.35 9.07 10.54 2.27 1.15 0.21 0.20 0.48 0.21 2.19 3.01 1.17 37.29 5.72 43.01 86.69 Lower 95% -1.59 -2.30 3.17 -6.32 2.52 -0.84 -0.99 -0.31 -0.22 -0.42 -0.13 0.67 -0.56 -2.91 Upper 95% 6.57 10.75 13.45 24.30 18.30 5.28 3.28 0.63 0.56 1.29 0.51 3.65 5.70 1.97 Mol % 6.78 11.41 22.40 24.33 28.28 6.08 3.09 0.58 0.54 1.27 0.57 5.87 8.06 48.28 latitude: 31° 17.0'N Extra amines longitude: 79° 46.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 8SA 1877 19954 4467 3343 3383 2306 125 556 125 777 125 732 2061 125 16571 8SB 979 3011 3557 2382 2408 1502 125 125 125 417 125 2502 1964 125 1913 8SC --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 1428.00 11482.5 4012.00 2862.50 2895.50 1904.00 125.00 340.50 125.00 597.00 125.00 1617.00 2012.50 125.00 9242.00 Area Std. Error 449.00 8471.50 455.00 480.50 487.50 402.00 0.00 215.50 0.00 180.00 0.00 885.00 48.50 0.00 7329.00 Predicted Conc. (nM) 2.34 17.74 10.93 6.08 6.48 2.05 0.19 0.59 0.20 0.72 0.21 2.33 4.01 1.17 44.10 15.60 59.70 73.87 Lower 95% 0.60 -10.82 7.85 3.27 3.19 0.87 -0.01 -0.42 -0.22 0.01 -0.13 -0.54 2.04 -2.91 Upper 95% 4.00 46.38 14.01 8.51 9.43 3.12 0.37 1.49 0.56 1.33 0.51 5.15 5.19 1.97 Mol % 5.30 40.24 24.78 13.79 14.69 4.64 0.42 1.33 0.45 1.62 0.48 5.29 9.09 40.82 latitude: 31° 17.0'N Extra amines longitude: 79° 46.0'W Asp-Lys sample depth: 50 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 8BA 435 3852 3561 1238 2739 1196 125 125 125 125 125 1964 1707 125 3809 8BB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 8BC 801 2162 4361 1095 2882 1426 125 125 125 688 125 2123 1699 125 4185 Area Mean 618.00 3007.00 3961.00 1166.50 2810.50 1311.00 125.00 125.00 125.00 406.50 125.00 2043.50 1703.00 125.00 3997.00 Area Std. Error 183.00 845.00 400.00 71.50 71.50 115.00 0.00 0.00 0.00 281.50 0.00 79.50 4.00 0.00 188.00 Predicted Conc. (nM) 1.01 4.65 10.79 2.48 6.29 1.41 0.19 0.21 0.20 0.49 0.21 2.95 3.39 1.17 24.64 6.75 31.39 78.51 Lower 95% 0.14 1.72 8.05 0.82 4.05 0.70 -0.01 -0.31 -0.22 -0.44 -0.13 2.45 1.42 -2.91 Upper 95% 1.79 7.51 13.53 3.49 8.18 2.00 0.37 0.63 0.56 1.32 0.51 3.40 4.52 1.97 Mol % 4.11 18.85 43.78 10.06 25.51 5.72 0.76 0.87 0.81 1.98 0.87 11.97 13.76 73.04 latitude: 31° 04.0'N Extra amines longitude: 79° 56.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 9SA 686 3483 4271 1973 2331 1113 125 125 125 503 125 2439 1665 125 2457 9SB --- 2349 3701 1301 1275 841 125 125 125 125 125 2413 1615 125 1934 9SC 1957 2986 3346 6723 4885 4001 792 1160 125 1228 125 1984 2037 125 3830 Area Mean 1321.50 2939.33 3772.67 3332.33 2830.33 1985.00 347.33 470.00 125.00 618.67 125.00 2278.67 1772.33 125.00 2740.33 Area Std. Error 635.50 328.19 269.42 1706.40 1071.61 1011.05 222.33 345.00 0.00 323.62 0.00 147.52 133.12 0.00 565.36 Predicted Conc. (nM) 2.16 4.54 10.28 7.08 6.33 2.14 0.52 0.81 0.20 0.74 0.21 3.29 3.53 1.17 32.72 4.63 37.35 87.62 Lower 95% -0.23 3.30 8.32 -1.17 0.58 -0.39 -0.25 -0.65 -0.22 -0.28 -0.13 2.65 1.46 -2.91 Upper 95% 4.47 5.72 12.21 15.02 11.75 4.56 1.27 2.17 0.56 1.68 0.51 3.88 4.78 1.97 Mol % 6.61 13.88 31.40 21.64 19.35 6.53 1.59 2.47 0.61 2.27 0.65 10.05 10.79 55.01 latitude: 31° 09.0'N Extra amines longitude: 80° 06.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 10SA 837 3875 3900 1336 6041 2794 437 125 125 566 125 2373 1580 125 8553 10SB 1035 4681 4509 1262 7026 2877 125 561 125 638 125 2259 1853 125 7456 10SC 1608 3829 4501 3782 6095 2768 663 125 125 474 125 2952 4874 125 10036 Area Mean 1160.00 4128.33 4303.33 2126.67 6387.33 2813.00 408.33 270.33 125.00 559.33 125.00 2528.00 2769.00 125.00 8681.67 Area Std. Error 231.18 276.65 201.68 827.94 319.71 32.87 155.97 145.33 0.00 47.46 0.00 214.54 1055.45 0.00 747.56 Predicted Conc. (nM) 1.90 6.38 11.72 4.52 14.29 3.03 0.61 0.46 0.20 0.67 0.21 3.65 5.51 1.17 42.60 14.65 57.25 74.41 Lower 95% 0.89 5.30 10.17 0.18 11.62 2.37 0.06 -0.32 -0.22 0.16 -0.13 2.83 0.20 -2.91 Upper 95% 2.83 7.42 13.31 8.36 16.76 3.58 1.15 1.15 0.56 1.10 0.51 4.42 10.18 1.97 Mol % 4.46 14.97 27.51 10.61 33.54 7.10 1.44 1.09 0.47 1.58 0.50 8.56 12.94 42.25 latitude: 31° 14.0'N Extra amines longitude: 80° 16.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 11SA --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 11SB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 11SC 3813 5740 3700 10925 9929 5389 1310 2585 125 1336 716 3211 2535 125 5330 Area Mean 3813.00 5740.00 3700.00 10925.0 9929.00 5389.00 1310.00 2585.00 125.00 1336.00 716.00 3211.00 2535.00 125.00 5330.00 Area Std. Error #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Predicted Conc. (nM) 6.24 8.87 10.08 23.22 22.21 5.80 1.96 4.44 0.20 1.60 1.22 4.63 5.05 1.17 86.62 9.00 95.61 90.59 Lower 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Upper 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Mol % 7.21 10.24 11.64 26.80 25.64 6.69 2.27 5.13 0.23 1.85 1.41 5.35 5.83 20.78 latitude: 31° 20.0'N Extra amines longitude: 80° 27.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 12SA 1733 4965 3742 2885 4672 2116 599 490 125 646 125 2493 1918 125 7668 12SB 1225 3845 3605 2431 3601 1725 125 125 125 644 125 2490 1795 125 5725 12SC --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 1479.00 4405.00 3673.50 2658.00 4136.50 1920.50 362.00 307.50 125.00 645.00 125.00 2491.50 1856.50 125.00 6696.50 Area Std. Error 254.00 560.00 68.50 227.00 535.50 195.50 237.00 182.50 0.00 1.00 0.00 1.50 61.50 0.00 971.50 Predicted Conc. (nM) 2.42 6.81 10.01 5.65 9.25 2.07 0.54 0.53 0.20 0.77 0.21 3.60 3.70 1.17 36.91 11.30 48.22 76.56 Lower 95% 1.34 4.83 9.04 3.73 5.81 1.26 -0.27 -0.37 -0.22 0.28 -0.13 3.17 1.71 -2.91 Upper 95% 3.43 8.75 10.94 7.15 12.42 2.77 1.34 1.32 0.56 1.18 0.51 3.98 4.87 1.97 Mol % 6.56 18.44 27.11 15.30 25.07 5.60 1.47 1.43 0.54 2.10 0.58 9.74 10.01 48.76 latitude: 31° 25.0'N Extra amines longitude: 80° 37.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 13SA 653 5075 3886 1190 2390 1435 376 125 125 388 125 1683 1445 125 5516 13SB 2199 3443 4575 6923 6958 4478 828 125 125 904 125 2152 1804 125 5196 13SC 1698 2362 3664 2412 3442 2070 397 125 125 619 125 2563 1821 125 3351 Area Mean 1516.67 3626.67 4041.67 3508.33 4263.33 2661.00 533.67 125.00 125.00 637.00 125.00 2132.67 1690.00 125.00 4687.67 Area Std. Error 455.41 788.54 274.26 1743.40 1381.13 926.81 147.29 0.00 0.00 149.23 0.00 254.22 122.60 0.00 674.69 Predicted Conc. (nM) 2.48 5.60 11.01 7.46 9.54 2.86 0.80 0.21 0.20 0.76 0.21 3.08 3.37 1.17 37.74 7.91 45.66 82.67 Lower 95% 0.73 2.87 9.04 -0.95 2.39 0.53 0.27 -0.31 -0.22 0.12 -0.13 2.15 1.30 -2.91 Upper 95% 4.16 8.29 12.99 15.58 16.40 5.10 1.32 0.63 0.56 1.33 0.51 3.96 4.59 1.97 Mol % 6.58 14.85 29.17 19.75 25.27 7.58 2.12 0.57 0.53 2.03 0.56 8.15 8.92 47.69 latitude: 31° 30.0'N Extra amines longitude: 80° 46.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 14SA 644 2326 3818 1005 2538 778 125 125 125 125 125 1617 1395 125 4178 14SB 2763 4470 4269 5950 5965 2748 1465 125 125 553 125 2337 2255 125 8126 14SC 2379 30826 3877 2449 5638 3193 1289 2690 371 1076 125 1287 1563 725 45137 Area Mean 1928.67 12540.7 3988.00 3134.67 4713.67 2239.67 959.67 980.00 207.00 584.67 125.00 1747.00 1737.67 325.00 19147.00 Area Std. Error 651.83 9163.59 141.53 1468.09 1091.92 742.04 420.41 855.00 82.00 274.99 0.00 310.00 263.17 200.00 13044.88 Predicted Conc. (nM) 3.16 19.38 10.86 6.66 10.54 2.41 1.44 1.68 0.33 0.70 0.21 2.52 3.46 3.03 55.53 32.32 87.85 63.21 Lower 95% 0.71 -11.51 9.61 -0.51 4.73 0.50 0.03 -1.68 -0.19 -0.21 -0.13 1.43 1.10 -4.05 Upper 95% 5.53 50.36 12.12 13.49 16.09 4.22 2.83 4.96 0.79 1.52 0.51 3.56 4.99 7.39 Mol % 5.69 34.89 19.56 12.00 18.99 4.34 2.59 3.03 0.60 1.26 0.38 4.54 6.23 32.41 latitude: 31° 35.0'N Extra amines longitude: 80° 57.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 15SA 2376 3718 3788 6241 8873 2549 508 125 125 717 598 2032 6479 125 12208 15SB 15326 147045 10552 15009 17481 12129 6270 15952 417 5564 1314 3887 6724 5110 178838 15SC 1558 3260 3147 2760 6463 1848 125 125 125 435 125 2440 1705 125 6530 Area Mean 6420.00 51341.0 5829.00 8003.33 10939.00 5508.67 2301.00 5400.67 222.33 2238.67 679.00 2786.33 4969.33 1786.67 65858.67 Area Std. Error 4459.26 47852.2 2368.74 3644.12 3344.17 3316.35 1987.58 5275.67 97.33 1664.66 345.62 562.80 1633.70 1661.67 56513.44 Predicted Conc. (nM) 10.51 79.34 15.88 17.01 24.47 5.93 3.45 9.28 0.36 2.69 1.16 4.02 9.90 16.68 184.78 111.16 295.93 62.44 Lower 95% -5.61 -81.85 0.55 0.12 8.10 -2.00 -3.12 -10.98 -0.20 -1.83 -0.22 2.16 2.27 -25.50 Upper 95% 26.64 241.21 31.40 34.33 40.83 13.81 10.00 29.54 0.85 7.14 2.49 5.84 17.29 60.19 Mol % 5.69 42.94 8.59 9.20 13.24 3.21 1.87 5.02 0.19 1.45 0.63 2.18 5.36 9.74 latitude: 31° 38.0'N Extra amines longitude: 81° 02.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 16SA 5714 71231 9032 5956 9764 5201 1816 7164 125 1595 125 2359 2695 3460 65844 16SB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 16SC 714 3716 3623 1162 6268 1532 125 125 125 489 125 2268 1843 125 5218 Area Mean 3214.00 37473.5 6327.50 3559.00 8016.00 3366.50 970.50 3644.50 125.00 1042.00 125.00 2313.50 2269.00 1792.50 35531.00 Area Std. Error 2500.00 33757.5 2704.50 2397.00 1748.00 1834.50 845.50 3519.50 0.00 553.00 0.00 45.50 426.00 1667.50 30313.00 Predicted Conc. (nM) 5.26 57.91 17.23 7.56 17.93 3.62 1.45 6.26 0.20 1.25 0.21 3.34 4.52 16.73 126.26 59.97 186.23 67.80 Lower 95% -3.81 -55.81 -0.25 -3.86 9.14 -0.82 -1.35 -7.28 -0.22 -0.34 -0.13 2.89 1.68 -25.59 Upper 95% 14.29 172.10 34.96 18.72 26.60 7.98 4.24 19.77 0.56 2.76 0.51 3.74 6.62 60.40 Mol % 4.17 45.86 13.65 5.99 14.20 2.87 1.15 4.96 0.16 0.99 0.17 2.64 3.58 14.26 latitude: 31° 24.0'N Extra amines longitude: 81° 09.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 17SA --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 17SB 2067 5001 3728 6198 10068 3204 1144 1819 125 698 125 2289 1861 125 4036 17SC 1261 6584 3854 2887 10677 2594 672 1040 125 960 125 2219 1788 125 5637 Area Mean 1664.00 5792.50 3791.00 4542.50 10372.5 2899.00 908.00 1429.50 125.00 829.00 125.00 2254.00 1824.50 125.00 4836.50 Area Std. Error 403.00 791.50 63.00 1655.50 304.50 305.00 236.00 389.50 0.00 131.00 0.00 35.00 36.50 0.00 800.50 Predicted Conc. (nM) 2.72 8.95 10.33 9.65 23.20 3.12 1.36 2.46 0.20 0.99 0.21 3.25 3.63 1.17 60.93 8.16 69.09 88.19 Lower 95% 1.15 6.22 9.38 1.73 20.64 2.13 0.55 0.85 -0.22 0.38 -0.13 2.81 1.66 -2.91 Upper 95% 4.23 11.66 11.26 17.46 25.73 4.01 2.16 3.99 0.56 1.53 0.51 3.65 4.79 1.97 Mol % 4.47 14.69 16.95 15.84 38.08 5.12 2.23 4.03 0.33 1.63 0.35 5.34 5.96 29.54 latitude: 31° 21.0'N Extra amines longitude: 81° 04.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 18SA --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 18SB 3429 4685 3054 11535 8380 5630 1818 2609 125 1171 548 2537 2056 125 3866 18SC --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 3429.00 4685.00 3054.00 11535.0 8380.00 5630.00 1818.00 2609.00 125.00 1171.00 548.00 2537.00 2056.00 125.00 3866.00 Area Std. Error #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Predicted Conc. (nM) 5.62 7.24 8.32 24.51 18.75 6.06 2.72 4.48 0.20 1.41 0.93 3.66 4.09 1.17 80.84 6.52 87.36 92.53 Lower 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Upper 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Mol % 6.95 8.96 10.29 30.32 23.19 7.49 3.37 5.55 0.25 1.74 1.16 4.53 5.06 22.27 latitude: 31° 16.0'N Extra amines longitude: 80° 54.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 19SA --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 19SB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 19SC 7392 8524 3214 24401 17036 11936 3017 8396 125 3392 1341 3645 4147 425 8595 Area Mean 7392.00 8524.00 3214.00 24401.0 17036.0 11936.0 3017.00 8396.00 125.00 3392.00 1341.00 3645.00 4147.00 425.00 8595.00 Area Std. Error #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Predicted Conc. (nM) 12.10 13.17 8.75 51.85 38.11 12.84 4.52 14.43 0.20 4.07 2.29 5.26 8.26 3.97 171.07 14.51 185.58 92.18 Lower 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Upper 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Mol % 7.08 7.70 5.12 30.31 22.28 7.50 2.64 8.44 0.12 2.38 1.34 3.07 4.83 10.52 latitude: 31° 11.0'N Extra amines longitude: 80° 45.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 20SA 1306 1781 4050 2119 4639 1788 125 125 125 468 125 2383 1388 381 6156 20SB 2734 4144 4018 6352 4978 3126 924 1379 125 799 125 2411 1946 125 6413 20SC 1021 3952 2948 2009 3104 833 125 125 125 125 125 2505 1855 125 6686 Area Mean 1687.00 3292.33 3672.00 3493.33 4240.33 1915.67 391.33 543.00 125.00 464.00 125.00 2433.00 1729.67 210.33 6418.33 Area Std. Error 529.93 757.70 362.12 1429.69 576.53 665.00 266.33 418.00 0.00 194.58 0.00 36.90 172.84 85.33 153.02 Predicted Conc. (nM) 2.76 5.09 10.00 7.42 9.49 2.06 0.59 0.93 0.20 0.56 0.21 3.51 3.44 1.96 38.23 10.83 49.06 77.92 Lower 95% 0.75 2.46 7.49 0.46 5.88 0.32 -0.32 -0.79 -0.22 -0.18 -0.13 3.07 1.30 -2.86 Upper 95% 4.70 7.67 12.49 14.10 12.81 3.70 1.48 2.56 0.56 1.20 0.51 3.91 4.76 3.75 Mol % 7.23 13.31 26.16 19.42 24.81 5.39 1.53 2.44 0.52 1.46 0.56 9.18 9.01 47.09 latitude: 31° 06.0'N Extra amines longitude: 80° 35.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 21SA 6628 73053 9150 8164 8645 8785 2664 3654 125 2875 722 3502 4271 1087 86452 21SB 3231 5557 3788 9832 6974 4625 1302 2475 125 1615 613 2462 2082 125 5210 21SC 405 2636 4355 682 2102 602 125 125 125 412 125 2170 1786 125 3760 Area Mean 3421.33 27082.0 5764.33 6226.00 5907.00 4670.67 1363.67 2084.67 125.00 1634.00 486.67 2711.33 2713.00 445.67 31807.33 Area Std. Error 1798.94 23001 1700.73 2813.51 1962.70 2362.34 733.59 1037.26 0.00 711.07 183.55 404.22 783.67 320.67 27325.54 Predicted Conc. (nM) 5.60 41.85 15.70 13.23 13.21 5.02 2.04 3.58 0.20 1.96 0.83 3.91 5.40 4.16 101.01 53.68 154.70 65.30 Lower 95% -0.94 -35.64 4.70 0.07 3.36 -0.65 -0.39 -0.46 -0.22 -0.04 0.04 2.54 1.22 -5.67 Upper 95% 12.10 119.65 26.89 26.54 22.85 10.64 4.46 7.56 0.56 3.88 1.58 5.24 8.93 11.60 Mol % 5.55 41.43 15.54 13.10 13.08 4.97 2.02 3.55 0.20 1.94 0.82 3.87 5.35 17.82 latitude: 31° 02.0'N Extra amines longitude: 80° 26.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 22SA 567 4460 3772 1132 2323 962 125 497 125 125 125 2430 1667 125 6283 22SB 2230 4096 3908 7177 5060 3303 1027 1442 125 740 125 2174 1736 125 5507 22SC 4300 5340 2091 14633 11723 7960 2456 3221 125 3229 1673 3959 4519 125 6970 Area Mean 2365.67 4632.00 3257.00 7647.33 6368.67 4075.00 1202.67 1720.00 125.00 1364.67 641.00 2854.33 2640.67 125.00 6253.33 Area Std. Error 1079.76 369.27 584.32 3904.49 2791.32 2056.70 678.61 798.54 0.00 948.92 516.00 557.26 939.38 0.00 422.59 Predicted Conc. (nM) 3.87 7.16 8.87 16.25 14.25 4.38 1.80 2.96 0.20 1.64 1.09 4.12 5.26 1.17 64.15 10.55 74.70 85.87 Lower 95% -0.09 5.80 4.95 -1.87 0.45 -0.58 -0.45 -0.18 -0.22 -0.99 -0.92 2.28 0.43 -2.91 Upper 95% 7.78 8.49 12.72 34.76 27.85 9.27 4.04 6.02 0.56 4.18 3.06 5.92 9.42 1.97 Mol % 6.04 11.16 13.83 25.34 22.21 6.83 2.81 4.61 0.31 2.55 1.70 6.42 8.20 28.06 latitude: 30° 55.0'N Extra amines longitude: 80° 04.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 23SA 1610 3322 5061 2580 3129 1566 513 125 125 605 125 2397 1834 125 5990 23SB 3055 5516 3764 11944 8953 5795 1342 1361 125 1054 691 3024 2389 125 8038 23SC 3626 4286 3246 11092 7640 5691 1209 1885 125 1164 665 2396 2107 125 6074 Area Mean 2763.67 4374.67 4023.67 8538.67 6574.00 4350.67 1021.33 1123.67 125.00 941.00 493.67 2605.67 2110.00 125.00 6700.67 Area Std. Error 599.92 634.90 539.79 2989.47 1763.71 1392.66 257.05 521.74 0.00 170.97 184.49 209.17 160.22 0.00 669.11 Predicted Conc. (nM) 4.53 6.76 10.96 18.15 14.71 4.68 1.53 1.93 0.20 1.13 0.84 3.76 4.20 1.17 63.58 11.31 74.89 84.90 Lower 95% 2.27 4.54 7.35 4.35 5.81 1.28 0.65 -0.17 -0.22 0.44 0.05 2.96 2.10 -2.91 Upper 95% 6.73 8.94 14.58 32.47 23.42 8.01 2.39 3.95 0.56 1.73 1.59 4.52 5.54 1.97 Mol % 7.12 10.63 17.24 28.54 23.13 7.36 2.41 3.04 0.31 1.78 1.32 5.91 6.61 28.31 latitude: 30° 55.0'N Extra amines longitude: 80° 04.0'W Asp-Lys sample depth: 20 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 23BA 707 3385 125 1639 4232 1367 336 125 125 550 125 2328 1752 125 6520 23BB 2258 4463 3335 3333 5568 1828 657 125 125 266 125 2477 1826 125 6756 23BC 1512 4613 3217 1897 9191 1724 125 781 125 125 125 2406 2007 125 9287 Area Mean 1492.33 4153.67 2225.67 2289.67 6330.33 1639.67 372.67 343.67 125.00 313.67 125.00 2403.67 1861.67 125.00 7521.00 Area Std. Error 447.84 386.76 1050.89 526.96 1481.42 139.60 154.67 218.67 0.00 124.98 0.00 43.03 75.74 0.00 885.62 Predicted Conc. (nM) 2.44 6.42 6.06 4.87 14.16 1.76 0.56 0.59 0.20 0.38 0.21 3.47 3.71 1.17 39.93 12.69 52.63 75.88 Lower 95% 0.71 5.00 -0.90 1.83 6.59 1.03 0.01 -0.42 -0.22 -0.23 -0.13 3.02 1.71 -2.91 Upper 95% 4.10 7.80 12.85 7.43 21.54 2.39 1.10 1.50 0.56 0.89 0.51 3.87 4.89 1.97 Mol % 6.12 16.07 15.18 12.18 35.46 4.42 1.40 1.48 0.50 0.94 0.53 8.69 9.28 45.08 latitude: 30° 50.0'N Extra amines longitude: 80° 04.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 24SA 2912 3230 7098 10978 7566 4773 953 1229 125 1131 554 3910 5777 125 6897 24SB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 24SC --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 2912.00 3230.00 7098.00 10978.0 7566.00 4773.00 953.00 1229.00 125.00 1131.00 554.00 3910.00 5777.00 125.00 6897.00 Area Std. Error #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Predicted Conc. (nM) 4.77 4.99 19.33 23.33 16.92 5.13 1.43 2.11 0.20 1.36 0.94 5.64 11.50 1.17 79.50 11.64 91.14 87.23 Lower 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Upper 95% #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Mol % 6.00 6.28 24.32 29.34 21.29 6.46 1.80 2.66 0.25 1.71 1.19 7.10 14.47 22.64 latitude: 30° 50.0'N Extra amines longitude: 80° 04.0'W Asp-Lys sample depth: 15 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 24BA 5687 8633 4873 13045 10702 6935 1747 3029 462 1610 778 3006 2297 125 20523 24BB 2327 4803 3611 4984 6233 4541 595 1682 125 1721 125 2754 2512 125 16144 24BC 1118 4021 4752 2108 5280 2585 591 479 125 1756 276 1605 5594 125 29531 Area Mean 3044.00 5819.00 4412.00 6712.33 7405.00 4687.00 977.67 1730.00 237.33 1695.67 393.00 2455.00 3467.67 125.00 22066.00 Area Std. Error 1366.81 1424.99 402.02 3273.37 1671.30 1257.86 384.67 736.51 112.33 44.01 197.37 431.18 1064.98 0.00 3940.75 Predicted Conc. (nM) 4.98 8.99 12.02 14.26 16.56 5.04 1.46 2.97 0.38 2.04 0.67 3.54 6.91 1.17 68.98 37.24 106.23 64.94 Lower 95% -0.01 4.15 9.29 -0.99 8.12 1.96 0.17 0.07 -0.21 1.52 -0.17 2.09 1.61 -2.91 Upper 95% 9.93 13.82 14.79 29.76 24.86 8.06 2.74 5.81 0.91 2.47 1.47 4.95 11.69 1.97 Mol % 7.23 13.03 17.42 20.68 24.01 7.31 2.12 4.31 0.55 2.95 0.97 5.14 10.01 26.09 latitude: 31° 46.0'N Extra amines longitude: 80° 43.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 25SA 2033 5830 4754 5748 5997 2848 771 1603 125 650 125 2647 1775 125 7155 25SB --- --- --- --- --- --- --- --- --- --- --- --- --- --- --- 25SC 713 3635 3914 797 3674 1098 125 125 125 125 125 2518 1804 125 6431 Area Mean 1373.00 4732.50 4334.00 3272.50 4835.50 1973.00 448.00 864.00 125.00 387.50 125.00 2582.50 1789.50 125.00 6793.00 Area Std. Error 660.00 1097.50 420.00 2475.50 1161.50 875.00 323.00 739.00 0.00 262.50 0.00 64.50 14.50 0.00 362.00 Predicted Conc. (nM) 2.25 7.31 11.80 6.95 10.82 2.12 0.67 1.49 0.20 0.47 0.21 3.73 3.56 1.17 40.95 11.47 52.41 78.12 Lower 95% -0.23 3.56 8.96 -4.86 4.69 -0.09 -0.42 -1.44 -0.22 -0.41 -0.13 3.25 1.60 -2.91 Upper 95% 4.65 11.04 14.69 18.45 16.69 4.23 1.75 4.32 0.56 1.26 0.51 4.16 4.70 1.97 Mol % 5.49 17.86 28.83 16.98 26.42 5.18 1.64 3.63 0.49 1.14 0.52 9.10 8.70 43.96 latitude: 31° 49.0'N Extra amines longitude: 80° 48.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 26SA 2148 6592 3776 5793 6878 3255 1066 125 125 832 125 2439 1855 125 6641 26SB 3312 7303 3908 9383 7988 4542 1306 1862 125 1124 692 2619 2318 125 6249 26SC 762 3177 3695 1047 4456 1113 125 125 125 556 125 2384 1956 125 4895 Area Mean 2074.00 5690.67 3793.00 5407.67 6440.67 2970.00 832.33 704.00 125.00 837.33 314.00 2480.67 2043.00 125.00 5928.33 Area Std. Error 737.05 1273.48 62.07 2414.10 1042.78 1000.07 360.39 579.00 0.00 163.99 189.00 70.97 140.56 0.00 528.91 Predicted Conc. (nM) 3.40 8.79 10.33 11.49 14.41 3.19 1.25 1.21 0.20 1.00 0.54 3.58 4.07 1.17 54.30 10.01 64.30 84.44 Lower 95% 0.65 4.46 9.39 0.13 8.85 0.70 0.04 -1.11 -0.22 0.33 -0.27 3.09 2.00 -2.91 Upper 95% 6.07 13.12 11.26 22.88 19.77 5.60 2.45 3.44 0.56 1.59 1.30 4.02 5.36 1.97 Mol % 6.26 16.20 19.03 21.17 26.53 5.88 2.30 2.23 0.37 1.85 0.99 6.59 7.49 33.15 latitude: 31° 51.0'N Extra amines longitude: 80° 53.0'W Asp-Lys sample depth: 6 m except NH4+ Asp Glu 8AAA Ser His/Thr/Gly Ala Tyr Arg Met Val Phe Ile Leu Lys Total except 8AAA(nM) except 8AAA Total amines(nM) %known 27SA 3868 9247 3875 10421 10417 7566 1969 2439 125 1060 608 2976 2238 125 10493 27SB 2790 5156 3369 7425 8338 4096 1396 1898 125 897 636 2396 2274 125 6463 27SC 4884 56299 3537 6339 10133 5942 1849 6757 125 1917 560 2902 2916 1122 50001 Area Mean 3847.33 23567.3 3593.67 8061.67 9629.33 5868.00 1738.00 3698.00 125.00 1291.33 601.33 2758.00 2476.00 457.33 22319.00 Area Std. Error 604.57 16408.4 148.79 1220.61 650.85 1002.39 174.47 1537.45 0.00 316.35 22.19 182.26 220.25 332.33 13889.81 Predicted Conc. (nM) 6.30 36.42 9.79 17.13 21.54 6.31 2.60 6.36 0.20 1.55 1.03 3.98 4.93 4.27 112.62 37.67 150.29 74.93 Lower 95% 4.04 -18.84 8.49 11.46 17.73 3.83 1.99 0.41 -0.22 0.55 0.67 3.25 2.73 -5.83 Upper 95% 8.53 91.94 11.05 23.26 25.28 8.75 3.21 12.26 0.56 2.47 1.34 4.67 6.44 12.01 Mol % 5.59 32.34 8.69 15.21 19.13 5.60 2.31 5.64 0.18 1.38 0.91 3.53 4.38 15.98 HPLC-HOH 125 125 125 125 125 125 125 125 125 125 125 2623 1529 125 HPLC-HOH 125 125 125 125 125 125 125 125 125 125 125 1846 993 125 HPLC-HOH --- --- --- --- --- --- --- --- --- --- --- --- --- --- Area Mean 125.00 125.00 125.00 125.00 125.00 125.00 125.00 125.00 125.00 125.00 125.00 2234.50 1261.00 125.00 Area Std. Error 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 388.50 268.00 0.00 Predicted Conc. (nM) 0.20 0.19 0.34 0.27 0.28 0.13 0.19 0.21 0.20 0.15 0.21 3.22 2.51 1.17 8.95 Lower 95% -0.33 -0.32 -0.58 -1.40 -1.97 -0.52 -0.01 -0.31 -0.22 -0.34 -0.13 1.90 0.10 -2.91 Upper 95% 0.64 0.61 0.87 1.11 2.08 0.65 0.37 0.63 0.56 0.55 0.51 4.50 4.00 1.97 Mol % 2.29 2.16 3.81 2.97 3.13 1.50 2.09 2.40 2.23 1.68 2.38 36.05 28.07 201.23